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How is the degree of crystallinity determined in DSC?
The degree of crystallinity may be determined from DSC by the comparison of crystallisation enthalpy of the investigated sample to the crystallisation enthalpy of the reference sample. Of course, one has to know exactly what is the degree of crystallinity of the reference sample (doesn't need to be fully amorphous).
What is the reason for non-standard DSC baseline shape?
As a result of testing the produced fibers, an additional peak was observed in the cooling and heating diagram. This is an interesting RG free document. What is the reason for non-standard DSC baseline shape? Greetings! We use thermogravimetric analyzer TGA/DSC 3+ (Mettler Toledo) to study clay minerals, soils and other objects.
What is the suitable parameters for salt hydrates DSC analysis?
We use subtracting of the DSC curve of the same sample heated to 1000°C, but its provided result is not ideal. Hello, I agree with Choon Fu Goh , try to check if the furnace is clean. Also, check the sensor if it is clean and not damaged. And you can also try to use a new crucible. What is the suitable parameters for salt hydrates DSC analysis ?
Last Update: Oct 2021
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Jermail
18.10.2021 00:46
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